反应详情

6-(3-Hexyl-2-hydroxyphenyl)-6′-(2-hydroxy-5-methoxyphenyl)-2,2′-bipyridine was prepared from 6-bromo-6′-(2-hydroxy-5-methoxyphenyl)-2,2′-bipyridine and 3-hexyl-2-hydroxyphenylboronic acid in 57% yield using method F; δH [2H6]-DMSO 12.40,(1H, s), 8.36,(2H, m), 8.25,(2H, t), 8.18,(1H, d), 8.09,(1H, d), 7.96,(1H, d), 7.65,(1H, s), 7.25,(1H, d), 6.99,(1H, d), 6.96-6.8,(2H, m), 3.81,(3H, s), 2.67,(2H, t), 1.60,(2H, m), 1.42-1.25,(6H, m), 0.88,(3H, t); MS 455 (MH)+; HPLC retention time (system 1) 4.96 minutes.

1. customHPLC retention time (system 1) 4.96 minutes