HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-bromobutanimide → 4-Bromo-5-(tert-butyl)isoxazol-3-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | 3-Isoxazolamine, 5-(1,1-dimethylethyl)- | HCID 171473 | — |
| Product | 4-Bromo-5-(tert-butyl)isoxazol-3-amine | HCID 15453199 | 91% |
Reaction Steps
This compound was prepared from 3-amino-5-tert-butylisoxazole and N-bromosuccinimide as described in Example 25a in 91% yield, Rf 0.27 (3:1 hexanes/ethyl acetate).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06541498B2 |
| Source dataset | uspto-grants-2003_04 |
| ORD ID | ord-364eb950dd21476dab546648150ed642 |
| Source note | uspto-grants-2003_04 |