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HRID1263825

反应详情

EQUATION

反应方程式

HRID 1263825 的结构方程式

REACTANTS

反应物

2
结构：O=C(O)CC1CCCC1
HCID71606

Cyclopentylacetic acid

C7H12O2

结构：CC(C)CN1C(=O)C(NC(=O)[C@H](C)N)C(=O)N(CC(C)C)c2ccccc21.Cl
HCID23552766

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)CN1C(=O)C(NC(=O)[C@H](C)NC(=O)CC2CCCC2)C(=O)N(CC(C)C)c2ccccc21
HCID22984229

未命名化合物

PROCEDURE

实验过程

Following General Procedure I above using cyclopentylacetic acid (Aldrich) and 3-(L-alaninyl)amino-2,4-dioxo-1,5-bis-(2-methylpropyl)-2,3,4,5-tetrahydro-1H-1,5-benzodiazepine hydrochloride (Example 8-S), the title compound was prepared as an amorphous white solid. Purification was by flash chromatography eluting with CH2Cl12/EtOAc (1:1). Rf=0.31 (CH2Cl2/EtOAc, 1:1).

WORKUP

后处理

  1. customPurification
  2. washeluting with CH2Cl12/EtOAc (1:1)