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HRID1263995

反应详情

EQUATION

反应方程式

HRID 1263995 的结构方程式

REACTANTS

反应物

2
结构：COc1ccc2c(c1)C(=O)C(=O)N2
HCID38333

1H-Indole-2,3-dione, 5-methoxy- (9CI)

C9H7NO3

结构：Cl.NNc1ccc(S(N)(=O)=O)cc1
HCID2794567

4-Hydrazinylbenzene-1-sulfonamide--hydrogen chloride (1/1)

C6H10ClN3O2S

PRODUCTS

生成物

1
结构：COc1ccc2c(c1)C(=NNc1ccc(S(N)(=O)=O)cc1)C(=O)N2
HCID178487247

未命名化合物

PROCEDURE

实验过程

The title compound was prepared from 5-methoxy-1H-indole-2,3-dione (Gassman, et al., Journal of Organic Chemistry 1977, 42, 1344-8) and 4-hydrazinobenzenesulfonamide hydrochloride according to Procedure G: mp>250° C.; 1H NMR (DMSO-d6): δ 3.80 (s, 3H), 6.87 (s, 2H), 7.20 (s, 1H), 7.28 (s, 2H), 7.60 (d, J=8.8 Hz, 2H), 7.81 (d, J=8.8 Hz, 2H), 10.93 (s, 1H), 12.85 (s, 1H); APCI−MS m/z 344.9 (M−H)−.