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HRID1264003

反应详情

EQUATION

反应方程式

HRID 1264003 的结构方程式

REACTANTS

反应物

2
结构：O=C1Nc2cc(Br)ccc2C1=O
HCID95716

1H-Indole-2,3-dione, 6-bromo-

C8H4BrNO2

结构：Cl.NNc1ccc(S(N)(=O)=O)cc1
HCID2794567

4-Hydrazinylbenzene-1-sulfonamide--hydrogen chloride (1/1)

C6H10ClN3O2S

PRODUCTS

生成物

1
结构：NS(=O)(=O)c1ccc(NN=C2C(=O)Nc3cc(Br)ccc32)cc1
HCID178514736

未命名化合物

PROCEDURE

实验过程

The title compound was prepared from 6-bromo-1H-indole-2,3-dione (Meth-Cohn and Goon, Tetrahedron Letters 1996, 37, 9381-4) and 4-hydrazinobenzenesulfonamide hydrochloride according to Procedure G: mp>250° C.; 1H NMR (DMSO-d6): δ 7.05 (s, 1H), 7.23 (d, J=8.1 Hz, 1H), 7.50 (d, J=8.1 Hz, 1H), 7.56 (d, J=8.7 Hz, 2H), 7.75 (d, J=8.7 Hz, 2H), 11.2 (s, 1H), 12.7 (s,1H); APCI−MS m/z 395 (M−H)−.