HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Amino-N-[3-(trifluoromethyl)phenyl]benzene-1-sulfonamide → HCID 178516999, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Amino-N-[3-(trifluoromethyl)phenyl]benzene-1-sulfonamide | HCID 232765 | — |
| Reactant | 8-[Ethoxymethylidene]-6H-[1,3]thiazolo[5,4-e]indol-7-one | HCID 53990807 | — |
| Product | HCID 178516999 | HCID 178516999 | 29% |
Reaction Steps
The title compound was prepared in 29% yield from 8-ethoxymethylene-6,8-dihydro-1-thia-3,6-diaza-as-indacen-7-one and N-(3-trifluoromethylphenyl)-4-aminobenzenesulfonamide according to Procedure J: 1H NMR (DMSO-d6): δ 11.2 (d, 1H), 10.9 (s, 1H), 10.7 (s, 1H), 9.3 (s, 1H), 8.1 (d, 1H), 7.8 (m, 3H), 7.5 (m, 4H), 7.1 (d, 1H); APCI−MS m/z 515 (M−H)−.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06541503B2 |
| Source dataset | uspto-grants-2003_04 |
| ORD ID | ord-cac5394004e048f9afc67815b63bf91c |
| Source note | uspto-grants-2003_04 |