HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfabenzamide → HCID 178517004, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfabenzamide | HCID 5319 | — |
| Reactant | 8-[Ethoxymethylidene]-6H-[1,3]thiazolo[5,4-e]indol-7-one | HCID 53990807 | — |
| Product | HCID 178517004 | HCID 178517004 | 25% |
Reaction Steps
The title compound was prepared in 25% yield from 8-ethoxymethylene-6,8-dihydro-1-thia-3,6-diaza-as-indacen-7-one and N-benzoyl-4-aminobenzenesulfonamide according to Procedure J: 1H NMR (DMSO-d6): δ 12.5 (br s, 1H), 11.2 (d, 1H), 10.9 (s, 1H), 9.3 (s, 1H), 8.1 (d, 1H), 8.0 (d, 2H), 7.9 (t, 3H), 7.65 (t, 3H), 7.5 (t, 2H), 7.2 (d, 1H); ESI−MS m/z 475 (M−H)−.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06541503B2 |
| Source dataset | uspto-grants-2003_04 |
| ORD ID | ord-ffe8d148a85343c595c7113951d366c6 |
| Source note | uspto-grants-2003_04 |