HuagongsheHuagongshe Chemistry Print Report · For research reference only
8-[Ethoxymethylidene]-6H-[1,3]thiazolo[5,4-e]indol-7-one → HCID 178516997, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 8-[Ethoxymethylidene]-6H-[1,3]thiazolo[5,4-e]indol-7-one | HCID 53990807 | — |
| Reactant | HCID 178507366 | HCID 178507366 | — |
| Product | HCID 178516997 | HCID 178516997 | 54% |
Reaction Steps
The title compound was prepared in 54% yield from 8-ethoxymethylene-6,8-dihydro-1-thia-3,6-diaza-as-indacen-7-one and 5-aminobenzotriazole according to Procedure J: 1H NMR (DMSO-d6): δ 11.18 (d,1H), 10.9 (s, 1H), 9.23 (s, 1H), 8.12 (d, 1H), 7.96 (s, 1H), 7.78 (d, 1H), 7.48 (s, 1H), 7.1 (d, 1H); APCI−MS m/z 333 (M−H)−.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06541503B2 |
| Source dataset | uspto-grants-2003_04 |
| ORD ID | ord-791a3951230746ef8ef7c692fc86c532 |
| Source note | uspto-grants-2003_04 |