HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chloro-3-nitrobenzoyl chloride → HCID 10309324, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chloro-3-nitrobenzoyl chloride | HCID 123477 | — |
| Reactant | Methyl 4-(4-aminophenyl)-4-oxobutanoate | HCID 12016833 | — |
| Product | HCID 10309324 | HCID 10309324 | 47.8% |
Reaction Steps
In a manner similar to that described in Example 3, 4-chloro-3-nitro-benzoyl chloride (0.073 g, 0.00033 mol) was allowed to react with 4-(4-amino-phenyl)-4-oxo-butyric acid, methyl ester (0.052 g, 0.00025 mol), and the resulting intermediate was hydrolyzed to give 0.045 g of 4-[4-(4-chloro-3-nitro-benzoylamino)-phenyl]-4-oxo-butyric acid as a yellow solid; MS-(AP+) MH+377.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06541521B1 |
| Source dataset | uspto-grants-2003_04 |
| ORD ID | ord-b0cc33b517f340e5bcee29dac236fcd2 |
| Source note | uspto-grants-2003_04 |