HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorotrimethylsilane → HCID 17961254, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorotrimethylsilane | HCID 6397 | — |
| Reactant | 8-Methyl-5,10-dihydroindeno[1,2-b]indole | HCID 22247079 | — |
| Reactant | Butyllithium | HCID 178418339 | — |
| Product | HCID 17961254 | HCID 17961254 | — |
Reaction Steps
The general procedure of Example A is followed. 8-Methyl-5, 10-dihydroindeno[1,2-b]indole reacts with n-butyllithium and the product then reacts with trimethylchlorosilane to form 5-trimethylsilyl-8-methyl-5, 10-dihydroindeno[1,2-b]indole. The later reacts with n-butyllithium to form a lithium salt, which reacts with zirconium tetrachloride to give Catalyst IV.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06541583B2 |
| Source dataset | uspto-grants-2003_04 |
| ORD ID | ord-e8fdc1c466a64d619104bf3a81372020 |
| Source note | uspto-grants-2003_04 |