HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 18618210, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | HCID 18618206 | HCID 18618206 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Solvent | N-methyl-2-pyrrolidone | HCID 13387 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 18618210 | HCID 18618210 | — |
Reaction Steps
To a stirred solution of acetyl chloride (0.16 g) in 1,4-dioxan (2 ml) was added a solution of the product from Example 7 (0.5 g) in pyridine (0.16 g) and N-methylpyrrolidinone (0.5 ml) and stirring was continued for 1 hour at room temperature. Water was added and the mixture was filtered to give a solid which was dried to give the title product, m.p. 273° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06541630B1 |
| Source dataset | uspto-grants-2003_04 |
| ORD ID | ord-fae58ac3016b46f9888a3a0b1c8d5d4e |
| Source note | uspto-grants-2003_04 |