Piperidine → HCID 18617713, compound

Participants

Role	Name	HCID	Charge
Reactant	Piperidine	HCID 8082	—
Reactant	N-[2-(3-Cyano-1H-indol-5-yl)-ethyl]-4-[2-chloropyrimidin-4-yl]benzamide	HCID 18617562	—
Product	HCID 18617713	HCID 18617713	—

Reaction Steps

Using piperidine and N-[2-(3-Cyano-1H-indol-5-yl)-ethyl]-4-[2-chloro-pyrimidin-4-yl]-benzamide (reference example 1az) as substrates. 1H NMR (DMSO) δ 1.6 (m, 6H); 2.98 (m, 2H); 3.55 (m, 2H); 3.84 (m, 4H); 7.19 (m, 2H); 7.49 (m, 2H); 7.93 (d, 2H, J=8 Hz); 8.20 (m, 31H); 8.44 (d, 1H, J=5 Hz); 8.69 (bt, 1H); 12.14 (bs, 1H). MS (ion spray) m/z 451 (M+H)+.

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US06541505B1
Source dataset	uspto-grants-2003_04
ORD ID	ord-b09030118c9a46d29244a57e66750a73
Source note	uspto-grants-2003_04