N-Methylethylamine → HCID 70029513, compound

Participants

Role	Name	HCID	Charge
Reactant	N-Methylethylamine	HCID 12219	—
Reactant	N-[2-(3-Cyano-1H-indol-5-yl)-ethyl]-4-[2-chloropyrimidin-4-yl]benzamide	HCID 18617562	—
Product	HCID 70029513	HCID 70029513	—

Reaction Steps

Using ethylmethylamine and N-[2-(3-Cyano-1H-indol-5-yl)-ethyl]-4-[2-chloro-pyrimidin-4-yl]-benzamide (reference example 1az) as substrates. 1H NMR (DMSO) δ 1.15 (t, 3H, J=7 Hz); 2.99 (bt, 2H); 3.17 (s, 3H); 3.56 (m, 2H); 3.73 (m, 2H); 7.20 (m, 2H); 7.50 (m, 2H); 7.94 (d, 2H, J=7 Hz); 8.20 (m, 3H); 8.44 (d, 1H, J=5 Hz); 8.69 (bs, 1H); 12.14 (bs, 1H). MS (ion spray) m/z 425 (M+H)+.

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US06541505B1
Source dataset	uspto-grants-2003_04
ORD ID	ord-503dda72b00b44fb9afbcd69a0d5fd98
Source note	uspto-grants-2003_04