Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Phenol | HCID 996 | — |
| Reactant | HCID 18618759 | HCID 18618759 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 9793984 | HCID 9793984 | — |
Reaction Steps
9.3 g (100 mmol) of phenol and 4.9 g (25 mmol) of 50% w/w difluoroacetaldehyde hydrate in water are introduced into a 100 ml reactor. 50 g of MgO are added. The mixture is stirred and is heated at 100° C. for 7 hours. The catalyst is filtered off.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06541674B2 |
|---|
| Source dataset | uspto-grants-2003_04 |
|---|
| ORD ID | ord-e56e1ff3477b463fbc0589c6c4b8382f |
|---|
| Source note | uspto-grants-2003_04 |
|---|
