HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium ethanethioate → HCID 86585041, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium ethanethioate | HCID 23670855 | — |
| Reactant | HCID 70004521 | HCID 70004521 | — |
| Reactant | HCID 86585042 | HCID 86585042 | — |
| Product | HCID 86585041 | HCID 86585041 | — |
Reaction Steps
(2S,4R)-4-Hydroxy-1-(naphthalene-2-sulfonyl)-pyrrolidine-2-carboxylic acid tert-butyl ester via (2S,4S)-4-Methanesulfonyloxy-1-(naphthalene-2-sulfonyl)-pyrrolidine-2-carboxylic acid tert-butyl ester which was treated with potassium thioacetate at 100° C. to give (2S,4R)-4-Acetylsulfanyl- 1-(naphthalene-2-sulfonyl)-pyrrolidine-2-carboxylic acid tert-butyl ester as light yellow solid, MS: 359 (M-HSCOCH3).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06541638B2 |
| Source dataset | uspto-grants-2003_04 |
| ORD ID | ord-2ad46aeb1991412795e03cf14a16fc5c |
| Source note | uspto-grants-2003_04 |