HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Phenylpropane-1-sulfonyl chloride → HCID 86585047, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Phenylpropane-1-sulfonyl chloride | HCID 12574631 | — |
| Reactant | HCID 70002487 | HCID 70002487 | — |
| Product | HCID 86585047 | HCID 86585047 | — |
Reaction Steps
Analogously, (2S,4R)-4-(2-[[4-(4-Methoxy-benzylsulfanyl)-pyrrolidine-2-carbonyl]-methyl-amino]-acetylamino)-benzoic acid ethyl ester was treated with 3-Phenyl-propane-1-sulfonyl chloride folowed by deprotection according to 8.1. to give (2S,4R)-4-[2-[[4-Mercapto-1-(3-phenyl-propane-1-sulfonyl)-pyrrolidine-2-carbonyl]-methyl-amino]-acetylamino]-benzoic acid ethyl ester as colorless foam MS: 548 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06541638B2 |
| Source dataset | uspto-grants-2003_04 |
| ORD ID | ord-8c56a12733994f6dbb83032667d93151 |
| Source note | uspto-grants-2003_04 |