HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → 1-Ethenyl-2-(iodomethyl)benzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Sodium Iodide | HCID 5238 | — |
| Reactant | 1-(Chloromethyl)-2-ethenylbenzene | HCID 89757 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | 1-Ethenyl-2-(iodomethyl)benzene | HCID 15830574 | 95% |
Reaction Steps
Dissolve 1-chloromethyl-2-vinyl-benzene (4.0 g, 26 mmol) in acetone (100 mL) and add sodium iodide (4.5 g, 30 mmol). Heat at gentle reflux for 30 minutes. Cool, add water (150 mL) and extract with pentane (200 mL). Dry (MgSO4) and evaporate the solvent in vacuo to give 1-iodomethyl-2-vinyl-benzene (95%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06544980B2 |
| Source dataset | uspto-grants-2003_04 |
| ORD ID | ord-62360d8ce7814f55b21d359d07ada96b |
| Source note | uspto-grants-2003_04 |