HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclopentylacetic acid → HCID 69270580, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclopentylacetic acid | HCID 71606 | — |
| Reactant | HCID 23552768 | HCID 23552768 | — |
| Product | HCID 69270580 | HCID 69270580 | — |
Reaction Steps
Following General Procedure I above using cyclopentylacetic acid (Aldrich) and 3-(L-alaninyl)-amino-2,4-dioxo-1,5-bis-(cyclopropylmethyl)-2,3,4,5-tetrahydro-1H-1,5-benzodiazepine hydrochloride (Example 8-U), the title compound was prepared as a white foam. Purification was by flash chromatography eluting with CH2Cl2/EtOAc (1:1 gradient to 2:3). Rf=0.50 (CH2Cl2/EtOAc, 1:1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06544978B2 |
| Source dataset | uspto-grants-2003_04 |
| ORD ID | ord-f9424d575e594b67b170f71e0d725528 |
| Source note | uspto-grants-2003_04 |