HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Fluoroaniline → HCID 9931758, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Fluoroaniline | HCID 9731 | — |
| Reactant | HCID 18613767 | HCID 18613767 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 9931758 | HCID 9931758 | 61.1% |
Reaction Steps
The same procedures as in Step 2 of Example 3 above were repeated using 5,6-dimethyl-2-chloro-4-(1-methyl-6-fluoro-1,2,3,4-tetrahydroisoquinolin-2-yl)pyrimidine (0.1 g, 0.33 mmol), dimethylformamide (5 ml), and 4-fluoroaniline (0.08 ml, 0.84 mmol) to afford 84 mg (61%) of the titled compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06545008B1 |
| Source dataset | uspto-grants-2003_04 |
| ORD ID | ord-1426fd8277d44634ac92213a05b93d4a |
| Source note | uspto-grants-2003_04 |