HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromomethyl 4-methoxyphenyl ketone → Methyl 4-[4-(4-methoxyphenyl)-2-oxazolyl]benzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromomethyl 4-methoxyphenyl ketone | HCID 4965 | — |
| Reactant | Methyl 4-carbamoylbenzoate | HCID 596094 | — |
| Product | Methyl 4-[4-(4-methoxyphenyl)-2-oxazolyl]benzoate | HCID 18613902 | 18% |
Reaction Steps
In the same manner as in Example 1, methyl 4-carbamoylbenzoate was reacted with 4-methoxyphenacyl bromide to obtain methyl 4-[4-(4-methoxyphenyl)-2-oxazolyl]benzoate. The product was recrystallized from ethanol. Yield: 18%. Pale yellow prisms. Melting Point: 200 to 202° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06545009B1 |
| Source dataset | uspto-grants-2003_04 |
| ORD ID | ord-2ca762ca8a294a8891e24d39223b101f |
| Source note | uspto-grants-2003_04 |