HRID1264945

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID2774185

2-Bromo-2',4'-difluoroacetophenone

C8H5BrF2O

HCID23279244

Methyl 3-carbamothioylbenzoate

C9H9NO2S

PRODUCTS

生成物

结构：COC(=O)c1cccc(-c2nc(-c3ccc(F)cc3F)cs2)c1

HCID18613919

未命名化合物

收率 69%

PROCEDURE

实验过程

In the same manner as in Example 28, methyl 3-thiocarbamoylbenzoate was reacted with 2,4-difluorophenacyl bromide to obtain methyl 3-[4-(2,4-difluorophenyl)-2-thiazolyl]benzoate. The product was recrystallized from ethanol. Yield: 69%. Pale yellow prisms. Melting point: 121 to 122° C.