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HRID1264947

反应详情

EQUATION

反应方程式

HRID 1264947 的结构方程式

REACTANTS

反应物

2
结构：O=C(CBr)c1ccc(F)c(F)c1
HCID2737032

2-Bromo-1-(3,4-difluorophenyl)ethan-1-one

C8H5BrF2O

结构：COC(=O)c1cccc(C(N)=S)c1
HCID23279244

Methyl 3-carbamothioylbenzoate

C9H9NO2S

PRODUCTS

生成物

1
结构：COC(=O)c1cccc(-c2nc(-c3ccc(F)c(F)c3)cs2)c1
HCID18613923

未命名化合物

收率 70%

PROCEDURE

实验过程

In the same manner as in Example 28, methyl 3-thiocarbamoylbenzoate was reacted with 3,4-difluorophenacyl bromide to obtain-methyl 3-[4-(3,4-difluorophenyl)-2-thiazolyl]benzoate. The product was recrystallized from ethanol. Yield: 70%. Colorless prisms. Melting point: 147 to 148° C.