HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromo-1-(4-tert-butylphenyl)ethan-1-one → Ethyl 3-[4-(4-t-butylphenyl)-2-thiazolyl]benzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromo-1-(4-tert-butylphenyl)ethan-1-one | HCID 2324770 | — |
| Reactant | Ethyl 3-thiocarbamoylbenzoate | HCID 18613909 | — |
| Product | Ethyl 3-[4-(4-t-butylphenyl)-2-thiazolyl]benzoate | HCID 18613859 | 37% |
Reaction Steps
In the same manner as in Example 74, ethyl 3-thiocarbamoylbenzoate was reacted with 4-t-butylphenacyl bromide to obtain ethyl 3-[4-(4-t-butylphenyl)-2-thiazolyl]benzoate. The product was recrystallized from ethanol. Yield: 37%. Pale yellow prisms. Melting point: 96 to 97° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06545009B1 |
| Source dataset | uspto-grants-2003_04 |
| ORD ID | ord-2dc80cedb8f34406b9b6b7ee7851b3dc |
| Source note | uspto-grants-2003_04 |