HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chlorothiobenzamide → HCID 18613811, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chlorothiobenzamide | HCID 2734826 | — |
| Reactant | Ethyl 4-(2-bromoacetyl)benzoate | HCID 11966043 | — |
| Product | HCID 18613811 | HCID 18613811 | 47% |
Reaction Steps
In the same manner as in Example 74, 4-chlorothiobenzamide was reacted with ethyl 4-bromoacetylbenzoate to obtain ethyl 4-[2-(4-chlorophenyl)-4-thiazolyl)benzoate. The product was recrystallized from ethanol. Yield: 47%. Pale yellow prisms. Melting point: 105 to 106° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06545009B1 |
| Source dataset | uspto-grants-2003_04 |
| ORD ID | ord-c708dad8b2324b5691e2f0001fe4df53 |
| Source note | uspto-grants-2003_04 |