HCID 10117716, compound → HCID 10141320, compound

HRID 1264970Notes

Reaction equation

HRID 1264970 reaction equation
[N:1]1[CH:6]=[CH:5][CH:4]=[C:3]([CH2:7][CH2:8][CH2:9][NH2:10])[CH:2]=1.N1(CCCN[C:21]([C@@H:23]2[CH2:28][CH2:27][CH2:26][CH2:25][N:24]2[S:29](=[O:44])(=[O:43])[NH:30][C:31]2[CH:36]=[C:35]([O:37][CH3:38])[C:34]([O:39][CH3:40])=[C:33]([O:41][CH3:42])[CH:32]=2)=[O:22])CCCCC1>>[N:1]1[CH:6]=[CH:5][CH:4]=[C:3]([CH2:7][CH2:8][CH2:9][NH:10][C:21]([C@@H:23]2[CH2:28][CH2:27][CH2:26][CH2:25][N:24]2[S:29](=[O:43])(=[O:44])[NH:30][C:31]2[CH:32]=[C:33]([O:41][CH3:42])[C:34]([O:39][CH3:40])=[C:35]([O:37][CH3:38])[CH:36]=2)=[O:22])[CH:2]=1

Participants

3

Reactant 2

HCID 10117716HCID 10117716, compoundHCID 135575233-(Pyridin-3-yl)propan-1-amine

Product 1

HCID 10141320HCID 10141320, compound

Procedure

Compound 93 was prepared from the carboxylic acid (compound 39) and 3-pyridin-3-yl-propylamine by a synthetic method analogous to the synthesis of compound 91. An 8.5% yield was obtained for the title compound.

Sources & evidence

ORD record
ord-50afdb527ac44923a9ae063a87d4d4a2
Source dataset
uspto-grants-2003_04
Patent number
US06544987B2

Reaction notes

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