m-Chloroperbenzoic acid → HCID 9820694, compound

Participants

Reaction Steps

To a solution of amine (1) (72 mg, 0.2 mmol) in CH2Cl2 (5 mL), m-CPBA (250 mg) was added. The reaction mixture was stirred at room temperature for 30 min. A solution of NaHCO3 (10 mL) was added and the organic layer was separated and washed with water (2×10 mL), dried (Na2SO4) and concentrated to obtain the title compound as a white solid.(43%); 1H NMR (CDCl3) δ 7.75 (2H, m), 3.6 and 4.4 (2H each, m); MS (M+) 370.

Provenance & Evidence