HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18615136, compound → HCID 18615154, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18615136 | HCID 18615136 | — |
| Reactant | Chloroform methanol | HCID 21584188 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 18615154 | HCID 18615154 | — |
Reaction Steps
According to the procedures as given in Example 2, the compound of Example 26 (in a solution of 200 mg of the compound in 25 ml of methanol) was subjected to a hydrogenolysis using 10% palladium/carbon black (100 mg), whereby the above-identified compound (153 mg) was obtained. Rf=0.09 (methanol/chloroform of 1/10).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06545053B1 |
| Source dataset | uspto-grants-2003_04 |
| ORD ID | ord-34f5269dae934682945ced11ae6c28aa |
| Source note | uspto-grants-2003_04 |