HuagongsheHuagongshe Chemistry Print Report · For research reference only
Nitric Acid → Ethyl 1-methyl-4-nitroimidazole-2-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Nitric Acid | HCID 944 | — |
| Reactant | 1-Methylimidazole | HCID 1390 | — |
| Reactant | Ethyl chloroformate | HCID 10928 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | Ethyl 1-methyl-4-nitroimidazole-2-carboxylate | HCID 2758876 | — |
Reaction Steps
Ethyl 1-methyl-4-nitroimidazole-2-carboxylate (10) was prepared by treatment of N-methylimidazole (16) with ethylchloroformate and triethylamine followed by nitration with nitric acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06545162B1 |
| Source dataset | uspto-grants-2003_04 |
| ORD ID | ord-c4a11db41582425897dc3b8dd9f8c94a |
| Source note | uspto-grants-2003_04 |