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HRID1265525

反应详情

EQUATION

反应方程式

HRID 1265525 的结构方程式

REACTANTS

反应物

2
结构：CNCC(C)C
HCID12249

1-Propanamine, N,2-dimethyl-

C5H13N

结构：CC(C)(C)OC(=O)Nc1cc(Cl)c(Cl)cc1[N+](=O)[O-]
HCID69489445

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)CN(C)c1cc(NC(=O)OC(C)(C)C)c([N+](=O)[O-])cc1Cl
HCID69489728

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CS(C)=O
溶剂HCID679

Dimethyl sulfoxide

C2H6OS

PROCEDURE

实验过程

The title compound was prepared from (4,5-dichloro-2-nitro-phenyl)-carbamic acid tert.-butyl ester (Example B2) (5.0 g, 16.3 mmol) and N-isobutyl-methylamine (7.09 g, 81.4 mmol) in DMSO (50 mL) at RT according to the general procedure C. Obtained as a brown oil (5.79 g, 99%).