HuagongsheHuagongshe Chemistry Print Report · For research reference only
Stannous chloride dihydrate → HCID 69687562, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Stannous chloride dihydrate | HCID 61436 | — |
| Reactant | (2-Dimethylamino-2',3'-difluoro-5-nitro-biphenyl-4-yl)-carbamic acid tert.-butyl ester | HCID 69688091 | — |
| Product | HCID 69687562 | HCID 69687562 | — |
Reaction Steps
The title compound was prepared from (2-dimethylamino-2′,3′-difluoro-5-nitro-biphenyl-4-yl)-carbamic acid tert.-butyl ester (Example D1) by reduction with SnCl2.2H2O according to the general procedure J (method b). Obtained as an orange solid (2.206 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06544985B2 |
| Source dataset | uspto-grants-2003_04 |
| ORD ID | ord-026df96a31af45098439c144e87c4bf3 |
| Source note | uspto-grants-2003_04 |