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HRID1265548

反应详情

EQUATION

反应方程式

HRID 1265548 的结构方程式

REACTANTS

反应物

1
结构：CN(C)c1cc(NC(=O)OC(C)(C)C)c([N+](=O)[O-])cc1C(F)(F)F
HCID69486578

未命名化合物

PRODUCTS

生成物

1
结构：CN(C)c1cc(NC(=O)OC(C)(C)C)c(N)cc1C(F)(F)F
HCID67362752

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：[Pd]
催化剂HCID23938

Palladium

Pd

PROCEDURE

实验过程

The title compound was prepared from (5-dimethylamino-2-nitro-4-trifluoromethyl-phenyl)-carbamic acid tert.-butyl ester (Example C4) by hydrogenation with 10% Pd/C according to the general procedure J (method a). Obtained as an amorphous yellow substance (1.34 g).

WORKUP

后处理

  1. customObtained as an amorphous yellow substance (1.34 g)