HuagongsheHuagongshe Chemistry Print Report · For research reference only
Stannous chloride dihydrate → Carbamic acid,[2-amino-4-chloro-5-[(2-methylpropyl)amino]phenyl]-,1,1-dimethylethyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Stannous chloride dihydrate | HCID 61436 | — |
| Reactant | (4-Chloro-5-isobutylamino-2-nitro-phenyl)-carbamic acid tert-butyl ester | HCID 69489292 | — |
| Product | Carbamic acid,[2-amino-4-chloro-5-[(2-methylpropyl)amino]phenyl]-,1,1-dimethylethyl ester | HCID 69489120 | — |
Reaction Steps
The title compound was prepared from (4-chloro-5-isobutylamino-2-nitro-phenyl)-carbamic acid tert-butyl ester (Example C31) (1.93 g, 5.61 mmol) by reduction with SnCl2.2H2O according to the general procedure J (method b). Obtained as a brown solid (1.30 g, 74%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06544985B2 |
| Source dataset | uspto-grants-2003_04 |
| ORD ID | ord-6d7f7eafdf6f483bb5fb4b4bccb8ab34 |
| Source note | uspto-grants-2003_04 |