HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 69689184, compound → (2-Amino-4-methyl-5-pyrrolidin-1-yl-phenyl)-carbamic acid tert-butyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 69689184 | HCID 69689184 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | (2-Amino-4-methyl-5-pyrrolidin-1-yl-phenyl)-carbamic acid tert-butyl ester | HCID 69688136 | — |
Reaction Steps
The title compound was prepared from (4-methyl-2-nitro-5-pyrrolidin-1-yl-phenyl)-carbamic acid tert-butyl ester (Example C36) (3.27 g, 10.2 mmol) by hydrogenation with 10% Pd/C according to the general procedure J (method a). Obtained as a pale brown solid (2.48 g, 83%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06544985B2 |
| Source dataset | uspto-grants-2003_04 |
| ORD ID | ord-4f5f917abae34cae933b9da202d840d6 |
| Source note | uspto-grants-2003_04 |