HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 3-(1H-1,2,4-triazol-1-YL)benzoate → 3-Oxo-3-(3-[1,2,4]triazol-1-yl-phenyl)-propionic acid tert-butyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 3-(1H-1,2,4-triazol-1-YL)benzoate | HCID 22224836 | — |
| Reactant | Lithium Tert-butyl Acetate | HCID 86586795 | — |
| Product | 3-Oxo-3-(3-[1,2,4]triazol-1-yl-phenyl)-propionic acid tert-butyl ester | HCID 69592807 | — |
Reaction Steps
The title compound was prepared from methyl 3-[1,2,4]triazol-1-yl-benzoate [CAS-No. 167626-27-9] by treatment with lithium tert.-butyl acetate according to general procedure K (method b). Obtained as an orange liquid (2.41 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06544985B2 |
| Source dataset | uspto-grants-2003_04 |
| ORD ID | ord-669f9dbaa5114adba0bdb02c3ee07ede |
| Source note | uspto-grants-2003_04 |