HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 18613374, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 86586812 | HCID 86586812 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 18613374 | HCID 18613374 | — |
Reaction Steps
The title compound was prepared from {4-chloro-2-[3-(2-cyano-pyridin-4-yl)-3-oxo-propionylamino]-5-dimethylamino-phenyl}-carbamic acid tert.-butyl ester (Example M15) by treatment with TFA in CH2Cl2 according to the general procedure N. Obtained as a yellow solid (50 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06544985B2 |
| Source dataset | uspto-grants-2003_04 |
| ORD ID | ord-970fe73105444c78bc6f728252b621cb |
| Source note | uspto-grants-2003_04 |