HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,5-Diaminobenzoic acid → 3,5-Bis({[(9H-fluoren-9-yl)methoxy]carbonyl}amino)benzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,5-Diaminobenzoic acid | HCID 12062 | — |
| Reactant | 9-Fluorenylmethyl chloroformate | HCID 34367 | — |
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Solvent | Water | HCID 962 | — |
| Product | 3,5-Bis({[(9H-fluoren-9-yl)methoxy]carbonyl}amino)benzoic acid | HCID 18547302 | — |
Reaction Steps
The compound was synthesised from 3,5-diaminobenzoic acid and Fmoc-chloride using sodium bicarbonate as base in a mixture of water and a suitable organic solvent. NMR analytical data were in accordance with the structure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06548048B1 |
| Source dataset | uspto-grants-2003_04 |
| ORD ID | ord-da5378e9e493428dbeb38bb398fcd220 |
| Source note | uspto-grants-2003_04 |