Thionyl Chloride → HCID 69701695, compound
Reaction equation
O[CH:2]([C:7]1[CH:12]=[CH:11][C:10]([C:13]2[N:18]3[CH2:19][CH2:20][C:21]4[NH:22][C:23](=[O:26])[CH:24]=[CH:25][C:16]([C:17]=43)=[CH:15][N:14]=2)=[CH:9][CH:8]=1)[CH2:3][CH:4]([CH3:6])[CH3:5].S(Cl)([Cl:29])=O>>[Cl:29][CH:2]([C:7]1[CH:12]=[CH:11][C:10]([C:13]2[N:18]3[CH2:19][CH2:20][C:21]4[NH:22][C:23](=[O:26])[CH:24]=[CH:25][C:16]([C:17]=43)=[CH:15][N:14]=2)=[CH:9][CH:8]=1)[CH2:3][CH:4]([CH3:6])[CH3:5]Participants
3
Procedure
This compound was prepared from intermediate 228 and thionyl chloride according to the procedure used in Example 171. Received 8.36 g (91%)
Sources & evidence
- ORD record
- ord-e24001d3ac3e4446a19b99c201c6a44e
- Source dataset
- uspto-grants-2003_04
- Patent number
- US06548494B1
Reaction notes
Loading…