Dimethylamine → HCID 69303173, compound

HRID 1266048Notes

Reaction equation

HRID 1266048 reaction equation
Cl[CH2:2][C:3]1[CH:8]=[CH:7][C:6]([C:9]2[N:14]3[CH2:15][C@@H:16]([CH2:23][OH:24])[C:17]4[NH:18][C:19](=[O:22])[CH:20]=[CH:21][C:12]([C:13]=43)=[CH:11][N:10]=2)=[CH:5][CH:4]=1.[CH3:25][NH:26][CH3:27]>C(#N)C>[CH3:25][N:26]([CH2:2][C:3]1[CH:8]=[CH:7][C:6]([C:9]2[N:14]3[CH2:15][C@@H:16]([CH2:23][OH:24])[C:17]4[NH:18][C:19](=[O:22])[CH:20]=[CH:21][C:12]([C:13]=43)=[CH:11][N:10]=2)=[CH:5][CH:4]=1)[CH3:27]

Participants

4

Reactant 2

HCID 674DimethylamineHCID 69702611HCID 69702611, compound

Product 1

HCID 69303173HCID 69303173, compound

Reagents, catalysts & solvents 1

HCID 6342AcetonitrileSolvent

Procedure

This compound was prepared from intermediate 238c and dimethylamine using the procedure described in Example 171, except with acetonitrile as solvent. Received 85.1 mg (33%).

Sources & evidence

ORD record
ord-9c142213a0e34a309f25ccb016da5388
Source dataset
uspto-grants-2003_04
Patent number
US06548494B1

Reaction notes

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