Dimethylamine → HCID 70009801, compound

HRID 1266049Notes

Reaction equation

Cl[CH:2]([C:4]1[CH:9]=[CH:8][C:7]([C:10]2[N:15]3[CH2:16][CH2:17][C:18]4[NH:19][C:20](=[O:23])[CH:21]=[CH:22][C:13]([C:14]=43)=[CH:12][N:11]=2)=[CH:6][CH:5]=1)[CH3:3].[CH3:24][NH:25][CH3:26]>>[CH3:24][N:25]([CH3:26])[CH:2]([C:4]1[CH:9]=[CH:8][C:7]([C:10]2[N:15]3[CH2:16][CH2:17][C:18]4[NH:19][C:20](=[O:23])[CH:21]=[CH:22][C:13]([C:14]=43)=[CH:12][N:11]=2)=[CH:6][CH:5]=1)[CH3:3]

Participants

Reactant 2

HCID 674Dimethylamine

HCID 69701328HCID 69701328, compound

Product 1

HCID 70009801HCID 70009801, compound

Conditions

Temperature: 80 °C

Procedure

This compound was prepared from intermediate 245b and dimethylamine according to the procedure described in Example 171, with the exception of heating to 80° C. Received 69 mg (77%)

Sources & evidence

ORD record: ord-19009312ab88405488fa4711c41740cb
Source dataset: uspto-grants-2003_04
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06548494B1

Reaction notes

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