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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1266424Generated: November 3, 2026

Dimethylformamide → HCID 18551249, compound

https://huagongshe.com/reaction/1266424

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDimethylformamideHCID 6228—
ReactantTri-o-tolylphosphineHCID 80271—
ReactantStannane, tributyl(1-ethoxyethenyl)-HCID 619414—
ReactantHCID 17935599HCID 17935599—
ProductHCID 18551249HCID 18551249—

Reaction Steps

Analogously to the compound above of 4-(4-bromo-3-methoxyphenyl)-2-hydroxy-4-methyl-2-trifluoromethyl-valeric acid ethyl ester, tributyl-1-ethoxyvinyltin, tri-o-tolylphosphine and bis-tri-o-tolylphosphine-palladium(II) chloride in dimethylformamide to 120° C., oil.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06548534B2
Source datasetuspto-grants-2003_04
ORD IDord-3bd6d7025ef946f3a942420ab70d1dea
Source noteuspto-grants-2003_04