HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromine → HCID 22708245, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromine | HCID 24408 | — |
| Reactant | 4-Bromothiophenol | HCID 66049 | — |
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | HCID 22708277 | HCID 22708277 | — |
| Product | HCID 22708245 | HCID 22708245 | — |
Reaction Steps
The synthesis was carried out similarly to Example II-1 from 4-bromothiophenol and 1,1-dimethylethyl 2-bromo-2-ethyl-butanoate [preparation, for example, similarly to Liebigs Ann. Chem. 725, 106-115 (1969); J. Am. Chem. Soc. 77, 946-947 (1955), and bromination with N-bromosuccinimide or bromine, for example similarly to Tetrahedron Lett. 1970, 3431; J. Org. Chem. 40, 3420 (1975)].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06548538B2 |
| Source dataset | uspto-grants-2003_04 |
| ORD ID | ord-135183f1fef6419babd25ec352a6c1cf |
| Source note | uspto-grants-2003_04 |