HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → Benzeneacetic acid, alpha-methyl-, ethyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Ethanol | HCID 702 | — |
| Reactant | 2-Phenylpropionic acid | HCID 10296 | — |
| Product | Benzeneacetic acid, alpha-methyl-, ethyl ester | HCID 99643 | — |
Reaction Steps
Dissolve 2-phenylpropionic acid (30 g) in 2B ethanol (100 mL and add anhydrous HCl (10 g). Allow to sit for 48-72 hours, evaporate the solvent in vacuo and purify by distillation to give ethyl 2-phenylpropionate (31 g); bp 100 C at 6 mm.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06548675B2 |
| Source dataset | uspto-grants-2003_04 |
| ORD ID | ord-c11446c89ba14e878adc3760584e893a |
| Source note | uspto-grants-2003_04 |