HuagongsheHuagongshe Chemistry Print Report · For research reference only
Morpholine → HCID 12048025, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Morpholine | HCID 8083 | — |
| Reactant | (5-Fluoro-2-nitro-4-trifluoromethyl-phenyl)-carbamic acid tert-butyl ester | HCID 12048024 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | HCID 12048025 | HCID 12048025 | — |
Reaction Steps
The title compound was prepared from (5-fluoro-2-nitro-4-trifluoromethyl-phenyl)-carbamic acid tert.-butyl ester (Example A1) (1.62 g, 5.0 mmol) and morpholine (2.18 mL, 25.0 mmol) in DMSO (10 mL) at 23° C. according to the general procedure B. Obtained as a yellow solid (1.83 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06548495B2 |
| Source dataset | uspto-grants-2003_04 |
| ORD ID | ord-f7f0f63c7f25413a958ebb06dfd7c518 |
| Source note | uspto-grants-2003_04 |