HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methoxyethanol → 5-(2-Methoxy-ethoxy)-2-nitro-4-pyrrol-1-yl-phenylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methoxyethanol | HCID 8019 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | 5-Chloro-2-nitro-4-pyrrol-1-yl-phenylamine | HCID 18548859 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | 5-(2-Methoxy-ethoxy)-2-nitro-4-pyrrol-1-yl-phenylamine | HCID 18548743 | — |
Reaction Steps
The title compound was prepared from 5-chloro-2-nitro-4-pyrrol-1-yl-phenylamine (Example F3) (1.01 g, 4 mmol), 2-methoxyethanol (1.58 mL, 20 mmol) and KOH (316 mg, 4.8 mmol) in DMSO (5 mL) according to the general procedure E. Obtained as an orange solid (870 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06548495B2 |
| Source dataset | uspto-grants-2003_04 |
| ORD ID | ord-9e9db5af966b4cfca83cab6f3020956a |
| Source note | uspto-grants-2003_04 |