HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → 5-Methoxy-2-nitro-4-pyrrol-1-yl-phenylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | 5-Chloro-2-nitro-4-pyrrol-1-yl-phenylamine | HCID 18548859 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | 5-Methoxy-2-nitro-4-pyrrol-1-yl-phenylamine | HCID 18548717 | — |
Reaction Steps
The title compound was prepared from 5-chloro-2-nitro-4-pyrrol-1-yl-phenylamine (Example F3) (5.94 g, 25 mmol), methanol (25 mL) and KOH (1.98 g, 30 mmol) in DMSO (25 mL) according to the general procedure E. Obtained as an orange solid (5.88 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06548495B2 |
| Source dataset | uspto-grants-2003_04 |
| ORD ID | ord-e6ee15db5ebc44d9980b62679a2b0bb5 |
| Source note | uspto-grants-2003_04 |