HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium hydride → 1-(3-Amino-4-nitro-phenyl)-4-phenyl-1H-pyrrole-3-carbonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | 5-Chloro-2-nitroaniline | HCID 74218 | — |
| Reactant | 4-Phenyl-1H-pyrrole-3-carbonitrile | HCID 3721460 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | 1-(3-Amino-4-nitro-phenyl)-4-phenyl-1H-pyrrole-3-carbonitrile | HCID 18548863 | — |
Reaction Steps
Prepared from 5-chloro-2nitroaniline, 4-phenyl-pyrrole-3-carbonitrile [CAS-no. 40167-37-1] and NaH in DMF at 150° C. for 3 h according to the general procedure E (method b). Obtained as a dark red solid (168 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06548495B2 |
| Source dataset | uspto-grants-2003_04 |
| ORD ID | ord-42cce114ea9f43d8a20c6174b0f6f50f |
| Source note | uspto-grants-2003_04 |