HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoic acid, 3-cyano-, methyl ester → 3-(3-Cyano-phenyl)-3-oxo-propionic acid tert-butyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoic acid, 3-cyano-, methyl ester | HCID 83554 | — |
| Reactant | Lithium Tert-butyl Acetate | HCID 86586795 | — |
| Product | 3-(3-Cyano-phenyl)-3-oxo-propionic acid tert-butyl ester | HCID 69592889 | — |
Reaction Steps
The title compound was prepared from methyl 3-cyanobenzoate [CAS-No. 13531-48-1] by treatment with lithium tert.-butyl acetate according to general procedure K (method b). Obtained as a light brown oily semisolid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06548495B2 |
| Source dataset | uspto-grants-2003_04 |
| ORD ID | ord-d0ecf21e24d34a0d97700b83f8d24715 |
| Source note | uspto-grants-2003_04 |