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HRID1266768

反应详情

EQUATION

反应方程式

HRID 1266768 的结构方程式

REACTANTS

反应物

3
结构：O=C(O)c1cccc(-n2ccnc2)c1
HCID2795544

3-(1H-imidazol-1-yl)benzoic acid

C10H8N2O2

结构：COC(=O)c1cccc(-n2ccnc2)c1
HCID22224641

未命名化合物

结构：CC(=O)OC(C)(C)C.[Li]
HCID86586795

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)(C)OC(=O)CC(=O)c1cccc(-n2ccnc2)c1
HCID69592789

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CO.O=S(=O)(O)O
溶剂HCID18363649

未命名化合物

PROCEDURE

实验过程

The title compound was prepared from methyl 3-(1H-imidazol-1-yl)benzoate [prepared from 3-(1H-imidazol-1-yl)benzoic acid (J. Med. Chem. 1987, 30, 1342; CAS-No. [108035-47-8] by refluxing in conc. H2SO4/MeOH] by treatment with lithium tert.-butyl acetate according to general procedure K (method b). Obtained as an orange-brown oil.

WORKUP

后处理

  1. customObtained as an orange-brown oil