Phosphoric Acid → HCID 20540603, compound

HRID 126680Notes

Reaction equation

HRID 126680 reaction equation
[CH3:1][CH:2]([CH:8]=[CH2:9])[CH2:3][CH2:4][CH2:5][CH2:6][OH:7].P(=O)(O)(O)O>>[CH2:8]([C:2]1([CH3:1])[CH2:3][CH2:4][CH2:5][CH2:6][O:7]1)[CH3:9]

Participants

3

Reactant 2

HCID 1004Phosphoric AcidHCID 543351HCID 543351, compound

Product 1

HCID 20540603HCID 20540603, compound

Procedure

1.8 grams of 5-methyl-6-hepten-1-ol (containing 5.4 percent 5-methyl-5-hepten-1-ol and 2.4 percent impurities) was reacted with 18 cc of 85 percent phosphoric acid at room temperature for 3.5 hours. Then the solution was worked up using the procedure of Example II. The v.p.c. showed the following to be present:

Sources & evidence

ORD record
ord-1153ac3659b5422d95fcf27dbcde7c5a
Source dataset
uspto-grants-1981_03
Patent number
US04254037

Reaction notes

Loading…