HuagongsheHuagongshe Chemistry Print Report · For research reference only
(2-Amino-5-chloro-4-trifluoromethyl-phenyl)-carbamic acid tert-butyl ester → HCID 86587000, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (2-Amino-5-chloro-4-trifluoromethyl-phenyl)-carbamic acid tert-butyl ester | HCID 69489727 | — |
| Reactant | 3-Oxo-3-(3-[1,2,3)triazol-1-yl-phenyl)-propionic acid ethyl ester | HCID 69592868 | — |
| Product | HCID 86587000 | HCID 86587000 | — |
Reaction Steps
The title compound was prepared from (2-amino-5-chloro-4-trifluoromethyl-phenyl)-carbamic acid tert-butyl ester (Example J14) (311 mg, 1.0 mmol) 3-oxo-3-(3-[1,2,3]triazol-1-yl-phenyl)-propionic acid ethyl ester (Example K1) (259 mg, 1.0 mmol) according to the general procedure M. Obtained as a light yellow oil (340 mg, 65%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06548495B2 |
| Source dataset | uspto-grants-2003_04 |
| ORD ID | ord-6bef0e9d41c441c6bd5e478c1724fa69 |
| Source note | uspto-grants-2003_04 |